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Free Content An efficient, large-scale synthesis of cytenamide

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Dibenzosuberenone (5H-dibenzo[a,d]cyclohepten-5-one) was reduced to the corresponding alcohol by sodium borohydride/MeOH and converted to the corresponding 5-chloro compound by thionyl chloride/benzene, treatment of which with CuCN/toluene gave the corresponding nitrile. Hydrolysis by ethanolic KOH yielded the corresponding amide, cytenamide (5H-dibenzo[a,d]cycloheptene-5-carboxamide).
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Keywords: 5H-5-CHLORODIBENZO[A,D]CYCLOHEPTENE; 5H-5-CYANODIBENZO[A,D]CYCLOHEPTENE; 5H-DIBENZO[A,D]CYCLO HEPTENE-5-CARBOXAMIDE; 5H-DIBENZO[A,D]CYCLOHEPTEN-5-ONE; CYTENAMIDE; DIBENZOSUBERENONE

Document Type: Research Article

Publication date: March 1, 2018

This article was made available online on March 28, 2018 as a Fast Track article with title: "An efficient, large-scale synthesis of cytenamide".

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  • Science Reviews 2000 is pleased to announce that the Journal of Chemical Research has been acquired by SAGE Publishing as of 7th December 2018. For more information, please visit https://uk.sagepub.com/en-gb/eur/sciencereviews2000

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