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Facile Synthesis and Characterization of Flower-Like PbS Microstructure via a Solvothermal Route

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PbS flowers were successfully synthesized by a simple solvothermal route. X-ray diffraction (XRD), scanning electron microscopy (SEM) showed that the as-prepared PbS microcrystals had a cubic structure and exhibited a beautiful six-petal flower-shaped morphology. The acetic acid and the ratios between lead acetate and element sulfur play key role in controlling the flower-like PbS microstructure. Then, based on a series of reference experiments, a possible formation mechanism was discussed. Furthermore, the optical and fluorescence properties were also investigated.
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Keywords: CRYSTAL STRUCTURE; FLOWERS; OPTICAL PROPERTIES; SEMICONDUCTORS

Document Type: Short Communication

Publication date: March 1, 2014

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  • Nanoscience and Nanotechnology Letters (NNL) is a multidisciplinary peer-reviewed journal consolidating nanoscale research activities in all disciplines of science, engineering and medicine into a single and unique reference source. NNL provides the means for scientists, engineers, medical experts and technocrats to publish original short research articles as communications/letters of important new scientific and technological findings, encompassing the fundamental and applied research in all disciplines of the physical sciences, engineering and medicine.
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