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Preparation of Mirabilite Microparticles via the Anti-Solvent Recrystallization Process

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Mirabilite microparticles was prepared via the anti-solvent recrystallization process. The solvent-antisolvent system was constructed by adding saturated aqueous solution of mirabilite into absolute ethanol. The best mixing mode and the mixing ratio, the stirring time and the droplet acceleration were selected by single factor experiments. Scanning electron microscopy (SEM) was used to characterize the generated mirabilite microparticles. The optimal one-factor conditions were solvent-anti-solvent ratio of 1:4, stirring for 40 min and droplet acceleration of 2 mL·min−1. Under the optimal conditions, the mirabilite microparticles with complete hexahedral form and uniform surface were obtained, the average particle size was about 5 μm.
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Keywords: Anti-Solvent Recrystallization; Microparticle; Mirabilite; Single Factor Method

Document Type: Research Article

Affiliations: 1: Affiliated Kunshan Hospital, Jiangsu University, Kunshan 215300, P. R. China 2: College of Vanadium and Titanium, Panzhihua University, 617000, P. R. China

Publication date: May 1, 2020

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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