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pH-Mediated Synthesis and Mechanistic Study of Homogeneous Magnetic [email protected]3O4 Nanoparticles

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In this paper, we report a novel kind of pH-mediated homogeneous magnetic [email protected]3O4 nanoparticles prepared by facile one-pot synthesis. The nanostructure and surface element composition along with magnetism of the as-synthesized hybrid nanoparticles can be easily adjusted by pH value in synthetic process. Furthermore, XRD and XPS detections indicated that the two components in the nanoparticles are both independent and certain synergistic. Compared with magnetic silver nanoparticles prepared by traditional multi-step methods, the homogeneous [email protected]3O4 nanoparticles showed excellent monodispersity and stability. Moreover, corresponding formation mechanism of the homogeneous hybrid magnetic nanoparticles was demonstrated in detail. Catalytic application of the homogeneous hybrid nanoparticles prepared under different pH values also verified rationality of the formation mechanism from side. This research provides a general strategy for constructing and large-scale preparing homogeneous magnetic hybrid metal nanoparticles.
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Keywords: Homogeneous; Magnetic Hybrid Nanoparticles; Mechanistic Study; One-Pot; pH-Mediated

Document Type: Research Article

Affiliations: 1: College of Chemistry and Molecular Engineering, Nanjing Tech University, Nanjing 210009, China 2: New Materials Research Institute, Yacoo Science, Suzhou, 215125, China

Publication date: April 1, 2020

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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