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Ball Milling of Copper Powder Under Dry and Surfactant-Assisted Conditions—On the Way Towards Cu/Cu2O Nanocatalyst

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Samples of copper powder was milled with varied grinding frequencies in the presence of various organic agents (oleylamine, ethylene glycol or dimethyl sulfoxide) or without additives. The effects of experimental conditions were investigated by X-ray diffractometry, scanning electron microscopy and dynamic light scattering measurements. The aggregation of particles were supressed by added organics. The catalytic activities of the variously treated samples were measured in the Ullmanntype reaction of iodobenzene and 1H-pyrazole.
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Keywords: Aggregation Suppression by Organics; Cu Powder; Dry or Wet Milling; Ullmann Reaction; XRD-SEM-DLS

Document Type: Research Article

Affiliations: 1: Department of Organic Chemistry, University of Szeged, Szeged, H-6720, Hungary 2: Department of Applied and Environmental Chemistry, University of Szeged, Szeged, H-6720, Hungary 3: Material and Solution Structure Research Group, University of Szeged, Szeged, H-6720, Hungary

Publication date: January 1, 2019

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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