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Crystal Structure Determination of the S/TiO2 System and the Correlation with Its Photocatalytic Properties

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A sulfur doped anatase photocatalyst was synthesized through a microwave-assisted sol–gel method and posteriorly, it was characterized using X-ray diffraction by powders (XRD) and High Resolution Electron Microscopy (HREM). Morphology and average size of the crystallite were determined for the sample, preferential crystal orientation was also analyzed and all these structural features were related to the photocatalytic properties. Moreover, a pure TiO2 sample was also obtained by the same synthesis method and it was used as a reference, and its structure and photocatalytic properties were compared to those observed for the sulfur doped anatase. The structural analysis showed similar results for both sample types but, photocatalytic properties are rather different. A small difference in chemical composition had an impact in the catalytic properties.
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Document Type: Research Article

Publication date: January 1, 2016

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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