Preparation and Photocatalytic of Nanoneedle Bi/ZnWO4 by Two-Step Hydrothermal Method
Nanoneedle Bi/ZnWO4 photocatalysts were successfully synthesized using a two-step hydrothermal method. In the first hydrothermal experiment ZnO/ZnWO4 nanoneedle crystals were synthesized from NaWO4 ·2H2O and Zn(NO3)2
·6H2O, using polyacrylamide (PAM) as a template in a hydrothermal environment. Bi cations were then reduced by t-BuONa in a second hydrothermal experiment, adding nanoneedle ZnO/ZnWO4. The catalysts were then characterized by powder X-ray diffraction (XRD), scanning
electron microcopy (SEM), energy dispersive spectrometer (EDS) and UV-vis diffuse reflectance spectrum (DRS). The results show that by adding Bi nanoparticles, the composition of the mixture gradually changed from that of ZnO/ZnWO4 to Bi/ZnWO4. The nanoneedle Bi/ZnWO4
samples displayed better UV light photocatalysis than the nanoneedle ZnO/ZnWO4 samples. The optimum concentration of Bi was investigated using a photocatalytic experiment. A “blue shift” was observed when the molar ratio of Bi was increased.
Document Type: Research Article
Publication date: 01 January 2016
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