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X-ray Study of Measured Thermal Properties of Ball Milled Metal Nanopowder

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Cadmium powder was ball milled in an argon inert atmosphere. The milled powders were characterized by X-ray diffraction. The high-energy ball milling of Cd after 25 hours resulted in particle size of 21 nm. Lattice strains in Cd powder produced by milling have been analyzed by X-ray powder diffraction. The lattice strain (ε) and Debye-Waller factor (B) are determined from the half-widths and integrated intensities of the Bragg reflections. Debye-Waller factor is found to increase with the lattice strain. From the correlation between the strain and effective Debye-Waller factors have been estimated for Cd. The variation of energy of vacancy formation as a function of lattice strain has been studied.
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Keywords: BALL MILLING; DEBYE-WALLER FACTOR; LATTICE STRAIN; PARTICLE SIZE; VACANCY FORMATION ENERGY; X-RAY DIFFRACTION

Document Type: Research Article

Publication date: December 1, 2014

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  • Journal of Advanced Physics is an interdisciplinary peer-reviewed journal consolidating research activities in all experimental and theoretical aspects of advanced physics. The journal aims in publishing articles of novel and frontier physics that merit the attention and interest of the whole physics community. JAP publishes review articles, full research articles, short communications of important new scientific and technological findings in all latest research aspects of physics.
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