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Exact One-Tailed 100p Upper Limits for Future Sample Repeatability Relative Standard Deviations Obtained in Single and Multilaboratory Repeatability Studies

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Formulas are derived to obtain exact one-tailed 100p upper limits (p and p) for future sample repeatability relative standard deviations, based on a noncentral t-distribution, for multi- and single-laboratory repeatability studies, respectively, used in the validation of analytical methods.
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Document Type: Research Article

Affiliations: 1: U.S. Food and Drug Administration, Center for Food Safety and Applied Nutrition, Office of Food Defense, Communication and Emergency Response, Division of Public Health and Biostatistics, Biostatistics Branch, 5100 Paint Branch Pkwy, College Park, MD 20740-3835. 2: U.S. Food and Drug Administration, Center for Food Safety and Applied Nutrition, Office of Food Defense, Communication and Emergency Response, Division of Public Health and Biostatistics, Biostatistics Branch, 5100 Paint Branch Pkwy, College Park, MD 20740-3835.

Publication date: November 1, 2007

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  • The Journal of AOAC INTERNATIONAL publishes refereed papers and reviews in the fields of chemical, biological and toxicological analytical chemistry for the purpose of showcasing the most precise, accurate and sensitive methods for analysis of foods, food additives, supplements and contaminants, cosmetics, drugs, toxins, hazardous substances, pesticides, feeds, fertilizers and the environment available at that point in time. The scope of the Journal includes unpublished original research describing new analytical methods, techniques and applications; improved approaches to sampling, both in the field and the laboratory; better methods of preparing samples for analysis; collaborative studies substantiating the performance of a given method; statistical techniques for evaluating data. The Journal will also publish other articles of general interest to its audience, e.g., technical communications; cautionary notes; comments on techniques, apparatus, and reagents.
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