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Accelerated Solvent Extraction of Fluometuron from Selected Soils

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Accelerated solvent extraction (ASE) is a recently developed extraction technique that is more rapid and produces less waste than do conventional liquid/liquid extraction methods. Optimal conditions were determined for ASE of fluometuron from 2 Weswood clay loam soils. Two solvents (acetonitrile and methanol), 2 temperatures (50 and 100C), and the number of static cycles (1, 2, and 3) were evaluated. The most efficient and reproducible extractions were obtained when methanol was combined with a 50C extraction temperature and the static cycle was repeated 3 times. These experiments indicated that existing extraction methods for fluometuron can easily be adapted for ASE.
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Document Type: Research Article

Affiliations: Texas A&M University, Soil and Crop Sciences, 2474 TAMU, 370 Olsen Blvd, College Station, TX 77843.

Publication date: July 1, 2007

More about this publication?
  • The Journal of AOAC INTERNATIONAL publishes refereed papers and reviews in the fields of chemical, biological and toxicological analytical chemistry for the purpose of showcasing the most precise, accurate and sensitive methods for analysis of foods, food additives, supplements and contaminants, cosmetics, drugs, toxins, hazardous substances, pesticides, feeds, fertilizers and the environment available at that point in time. The scope of the Journal includes unpublished original research describing new analytical methods, techniques and applications; improved approaches to sampling, both in the field and the laboratory; better methods of preparing samples for analysis; collaborative studies substantiating the performance of a given method; statistical techniques for evaluating data. The Journal will also publish other articles of general interest to its audience, e.g., technical communications; cautionary notes; comments on techniques, apparatus, and reagents.
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