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Liquid–liquid microextraction and spectrophotometric determination of anionic surfactants using Astra Phloxine FF

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A novel and simple procedure for determination of anionic surfactants has been developed. The method is based on the reaction of sodium dodecyl sulphate (SDS) with Astra Phloxine FF reagent at pH 3–8, followed by liquid–liquid microextraction of the formed ion associate into an organic phase containing a mixture of carbon tetrachloride and dichloroethane (4:1, v/v) and subsequent UV-Vis detection at 555 nm. The calibration plot was linear in the range 0.006–0.29 mg L−1 of SDS. The limit of detection (LOD), calculated based on 3s, is 0.002 mg L−1. The method was applied to the determination of anionic surfactants in real wastewater samples.
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Keywords: anionic surfactants; liquid–liquid microextraction; spectrophotometry; wastewater samples

Document Type: Research Article

Affiliations: 1: Department of Analytical Chemistry, Uzhorod National University, Uzhorod, UA,–88000, Ukraine 2: Department of Environmentalistics, Technical University in Košice, Košice, SK,–04200, Slovak Republic 3: Department of Analytical Chemistry, University of P.J. Šafárik, Košice, SK,–04154, Slovak Republic

Publication date: February 19, 2015

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