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Isolation and Characterization of Badge Hydrolysis Products

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Heating a suspension of Bisphenol A diglycidyl ether (BADGE) in 20 : 80 tetrahydrofuran/water at 70°C and subsequent passage of the resulting solution through C18 columns allowed isolation and purification to > 97% of each of the two hydrolysis products 2-[4-(2,3-dihydroxypropoxy) phenyl]-2-[4-(2,3-epoxypropoxy)phenyl]propane (1HP) and 2,2-bis[4-(2,3-dihydroxypropoxy)phenyl] propane (2HP), which were characterized by UV, IR, 1H and I3C NMR spectroscopy and mass spectrometry.
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Keywords: BADGE; BADGE hydrolysis products; Infrared spectroscopy; Mass spectrometry; Nuclear magnetic resonance; Ultraviolet spectroscopy

Document Type: Research Article

Affiliations: 1: Departamento de Química Analítica, Nutrición y Bromatología (A´rea de Nutrición y Bromatología), Facultad de Farmacia, Universidad de Santiago de Compostela, 15706 Santiago de Compostela, Spain 2: Departamento de Química Orgánica, Facultad de Farmacia, Universidad de Santiago de Compostela, 15706 Santiago de Compostela, Spain

Publication date: January 1, 2002

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