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Syntheses, structures and photocatalytic degradation of organic dyes for two isostructural copper coordination polymers involving in situ hydroxylation reaction

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Two copper(II) coordination polymers, {[Cu2(btre)(hsuc)Cl(H2O)]·1.5H2O}n (1) and {[Cu2(btre)(hsuc)Br(H2O)]·1.5H2O}n (2) (btre = 1,2-bis(1,2,4-triazol-4-yl)ethane, H3hsuc = 2-hydroxysuccinic acid), were synthesized by the hydrothermal method via in situ hydroxylation reaction with fumarate (fum), btre and CuCl2/CuBr2, and characterized by elemental analyses, IR, TG and X-ray diffraction. 1 and 2 are isostructural and show a 4-connected 2-D network based on [Cu2O] dimers. 1 and 2 show good photocatalytic activity for the degradation of organic dyes methylene blue and methyl orange under UV light irradiation.
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Keywords: Coordination polymer; copper(II) compound; fumarate; in situ hydroxylation; photocatalytic degradation

Document Type: Research Article

Affiliations: State and Local Joint Engineering Laboratory for Functional Polymeric Materials, College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou, P.R. China

Publication date: May 3, 2018

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