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Coordination compounds based on CAPh type ligand: synthesis, structural characteristics and luminescence properties of tetrakis-complexes CsLnL4 with dimethylbenzoylamidophosphate

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Searching for prospective luminescent materials, the series of new lanthanide coordination compounds CsLnL4 (Ln = La, Pr, Nd, Sm – Er, and Yb; L = {C6H5CONPO(OCH3)2}-) was synthesized. X-ray diffraction studies of CsNdL4 and CsYbL4 have been performed establishing polymeric structures of the tetrakis-complexes built from [LnL4] anions and cesium cations functioning as linkers. The IR, absorption, emission, excitation spectra, and decay time measurements at 298 and 77 K, as well as thermal gravimetric analyses, were used to characterize the complexes.
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Keywords: Carbacylamidophosphates; crystal structure; lanthanides; luminescence; tetrakis-complexes

Document Type: Research Article

Affiliations: 1: Department of Chemistry, Kyiv National Taras Shevchenko University, Kyiv, Ukraine 2: National Academy of Science of Ukraine, STC “Institute for Single Crystals”, Khar’kov, Ukraine 3: National Academy of Sciences of Ukraine, A.V. Bogatsky Physicochemical Institute, Odessa, Ukraine

Publication date: January 2, 2016

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