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Synthesis and characterization of a thioether Schiff base ligand and its metal complexes and crystal structure determination of the nickel(II) complex

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Reactions of 1,2-di(o-aminophenylthio)ethane with 3-ethoxy-2-hydroxybenzaldehyde yield the new hexadentate N2S2O2 donor thioether Schiff base 1,2-bis(2-((2-(thio)phenylimino)methyl)-6-ethoxyphenol)ethane (H2L). Ni(II), Zn(II), Cd(II), and Hg(II) complexes of this ligand were prepared. Of these complexes, [NiL]ยท2H2O has been structurally characterized by X-ray crystallography. The coordination geometry around Ni(II) was described as octahedral. Zn(II), Cd(II), and Hg(II) complexes and the Schiff base ligand have been characterized by CHN analyses, molar conductivity, UV–vis, FT-IR, 1H, and 13C NMR spectroscopy.
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Keywords: Hexadentate ligand; N2S2O2 donor; Nickel(II) complex; Schiff base complex; Thioether ligand

Document Type: Research Article

Affiliations: 1: Faculty of Science, Department of Chemistry, Yazd University, Yazd, Iran 2: Department of Chemistry, Payame Noor University, Tehran, Iran 3: Chemistry Department, Shahid Beheshti University, Tehran, Iran

Publication date: December 17, 2015

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