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Synthesis and physico-chemical study of complexation of glyoxylic acid aroylhydrazones with Cu(II) in solution and solid phase

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A series of copper(II) binuclear metallochelates with glyoxylic acid aroylhydrazones have been synthesized. The composition and structure were established with infrared, UV-Vis, 1H NMR, extended X-ray adsorption fine structure spectroscopy as well as magnetochemical studies and potentiometry. The proton-donor and proton-acceptor features of the ligand systems play a key role in the formation of the complexes.
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Keywords: Coordination compounds; EXAFS; Exchange interaction; Hydrazones; Magnetochemistry

Document Type: Research Article

Affiliations: 1: Department of Chemistry, Southern Federal University, Rostov-on-Don, 344090, Russian Federation 2: Southern Scientific Centre of RAS, Rostov-on-Don, 344006, Russian Federation 3: Institute of Physics, Rostov-on-Don, 344090, Russian Federation

Publication date: June 1, 2011

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