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Lead(II) complexes of o-phthalate including a crystal structure of a novel 2D coordination polymer, [Pb(pht)(H2O)]n

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Three new o-phthalate (pht) lead(II) complexes were synthesized and characterized by elemental analyses, IR, 1H NMR, and 13C NMR spectroscopy. Single crystal X-ray structural analysis of [Pb(pht)(H2O)]n shows the complex to be a novel 2D chain polymer as a result of phthalate bridging. Coordination number of Pb(II) is eight, PbO8, with a "stereo-chemically active" electron lone pair, and the coordination sphere is hemidirected. Packing of this compound in the solid state via - stacking and hydrogen bonding is discussed.
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Keywords: Crystal structure; Lead(II); Phthalate

Document Type: Research Article

Affiliations: 1: Department of Science, Payam Noor University of Zanjan, Zanjan, Iran 2: Department of Chemistry, Zanjan University, Zanjan, Iran

Publication date: July 1, 2007

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