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Copper(II) complexes with tetradentate imine-phenols: synthesis, characterization and molecular structures

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Four copper(II) complexes of N , N '-bis(4-methoxysalicylidene)-1,2-diimino ethanemonohydrate ( 1 ), N , N '-bis(5-methoxysalicylidene)-1,2-diiminoethane ( 2 ), N , N '-bis(3-methoxysalicylidene)-2,2-dimethyl-1,3-diiminopropane ( 3 ) and N , N '-bis(4-methoxysalicylidene)-2,2-dimethyl-1,3-diiminopropane ( 4 ) have been prepared and characterized spectroscopically. The solid-state structures of the complexes were established by X-ray crystallography. Complexes 2 , 3 and 4 contain Cu(II) in a tetrahedrally distorted square planar environment with two phenolate O atoms being deprotonated. Complex 1 is five-coordinate and displays color isomerism.
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Keywords: Copper; Imine-phenols; Molecular structures

Document Type: Research Article

Affiliations: 1: Department of Radiological Technology, Yuanpei University of Science and Technology, Hsinchu, Taiwan 300, ROC 2: Department of Nuclear Science, National Tsing Hua University, Hsinchu, Taiwan 300, ROC 3: Department of Chemistry, National Tsing Hua University, Hsinchu, Taiwan 300, ROC 4: Department of Chemistry, The University of Burdwan, Golapbag, Burdwan 713104, India

Publication date: July 20, 2005

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