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Crystal Structure and Magnetic Properties of a Copper(II) Chloride Complex with Nitronyl Nitroxide

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A new compound [Cu(NITPhCH3)2Cl2] (NITPhCH3 2-(4-methyl-phenyl)-4,4,5,5-tetramethyl-imidazoline-1-oxyl-3-oxide) has been characterized spectroscopically. A crystal structure analysis has shown the copper ion to be planar, coordinated by two chlorine atoms and two oxygen (nitroxyl) atoms. Based on magnetic susceptibility measurements the compound was found to exhibit a moderately strong antiferromagnetic interaction (J=−107.44 cm−1) between copper(II) and the radical.
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Keywords: Copper(II) complex; Crystal structure; Magnetic interactions; Nitronyl nitroxide

Document Type: Research Article

Affiliations: Department of Chemistry, Nankai University, Tianjin 300071, P.R. China

Publication date: January 1, 2002

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