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A novel steroidal glycoside, ophiofurospiside A from Ophiopogon japonicus (Thunb.) Ker-Gawl

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A new furospirostanol saponin, ophiofurospiside A (1), was isolated together with the known steroidal glycosides 2, 3, and 4 from the tubers of Ophiopogon japonicus (Thunb.) Ker-Gawl. Using chemical and spectral analyses (IR, MS, 1D NMR, and 2D NMR), the structure of 1 was established as 26-O--d-glucopyranosyl-(22S, 25R)-furospirost-5-ene-3, 17α, 26-triol-3-O-[α-l-rhamnopyranosyl-(1 → 2)]-[-d-xylopyranosyl-(1 → 4)]-glucopyranoside (1). Three known steroidal saponins 2-4 were identified on the basis of spectroscopic data.
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Keywords: Ophiopogon japonicus (L.f) Ker-Gawl; furospirostanol saponin; liliaceae; ophiofurospiside A

Document Type: Research Article

Affiliations: 1: Department of Traditional Chinese Medicine Chemistry, School of Traditional Chinese Medicine, Beijing University of Chinese Medicine, Beijing, China 2: Institute of Traditional Chinese Medicine, Academy of Traditional Chinese Medicine and Material Medica of Jilin Province, Changchun, China

Publication date: May 1, 2008

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