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Open Access Crystal structure of 1-[3,5-bis(trifluoromethyl)phenyl]-2-bromoethan-1-one

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The title compound, C10H5BrF6O, synthesized via continuous stirring of 3,5-bis(trifluoromethyl) acetophenone with bromine in an acidic medium and concentrated under reduced pressure, crystallizes with four molecules in the unit cell (Z = 4) and one formula unit in the asymmetric unit. In the crystal, molecules are linked in a head-to-tail fashion into dimers along the b-axis direction through weak C—H...Br and C—O...Csp2 interactions. C—H...O, C—F...π and F...F interactions are also observed.
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Document Type: Research Article

Affiliations: 1: Institute for Stem Cell Biology and Regenerative Medicine (inStem), GKVK Campus, Bellary Road, Bangalore 560 065, Karnataka, India 2: Department of Chemistry, Visvesvaraya National Institute of Technology, Nagpur 440010, Maharashtra, India 3: Department of Biotechnology and Food Technology, Faculty of Applied Science, Durban University of Technology, Durban 4001, South Africa

Publication date: January 1, 2018

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