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Open Access Crystal structure of 3-hydroxy-2-(4-hydroxy-3-methoxyphenylmethyl)-5,5-dimethylcyclohex-2-enone

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In the title compound, C16H20O4, a new starting compound for the synthesis of various heterocycles, the partially saturated six-membered ring adopts a sofa conformation. An intramolecular O—H...O hydrogen bond is observed in the guaiacol residue. In the crystal, molecules are assembled into a sheet structure parallel to the ab plane via O—H...O hydrogen bonds. The hydrogen-bond pattern is described by an R44(28) graph-set motif. The sheets are further linked by C—H...O hydrogen bonds into a three-dimensional network.
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Document Type: Research Article

Affiliations: 1: Institute of Technology of Organic Chemistry, Faculty of Materials Science and Applied Chemistry, Riga Technical University, P. Valdena Str. 3/7, Riga, LV-1048, Latvia 2: Latvian Institute of Organic Synthesis, Aizkraukles Str. 21, Riga, LV-1006, Latvia

Publication date: January 1, 2018

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