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Open Access Crystal structure of 2,3,5,6-tetrakis(pyridin-2-yl)pyrazine hydrogen peroxide 4.75-solvate

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The structure of the title co-crystal, C24H16N6·4.75H2O2, consists of a 2,3,5,6-tetrakis(pyridin-2-yl)pyrazine coformer and hydrogen peroxide solvent molecules in an overall ratio of 1:4.75. Three of the six H2O2 molecules modelled in the structure were found to be cross-orientationally disordered over two positions with occupancy ratios 0.846 (9):0.154 (9), 0.75 (2):0.25 (2), and 0.891 (9):0.109 (9). In the crystal, all of the peroxide molecules are linked into hydrogen-bonded chains that propagate parallel to the a axis. These chains are further linked by O—H...N hydrogen bonds to the pyridine groups of the main molecule.
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Document Type: Research Article

Affiliations: Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii prosp. 31, Moscow 119991, Russian Federation

Publication date: January 1, 2017

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