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Electron Energy Loss Spectroscopy Analysis on the Preferential Incorporation of Er 3+ Ions into Fluoride Nanocrystals in Oxyfluoride Glass‐Ceramics

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The preferential incorporation of Er 3+ ions into the PbF 2 nanocrystals during the ceraming process of oxyfluoride glass was analyzed using electron energy loss spectroscopy analysis. Concentrations of Er 3+ ions were considerably higher in PbF 2 nanocrystals compared to those in the glass matrix. Changes in lineshapes of absorption spectra from Er 3+: 4 I 15/24 I 13/2 transition and lifetimes of the excited‐state Er 3+ (4 S 3/2 level) ions also supported the incorporation of Er 3+ ions into PbF 2 nanocrystals.
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Document Type: Research Article

Publication date: July 1, 2012

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