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Quantitative Raman Analysis of Free Carbon in Polymer-Derived Ceramics

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Nanosized carbon clusters self-formed in polymer-derived ceramics (named free carbon) play a key role in determining the properties of the materials. However, it is difficult to quantitatively measure the concentration of the free carbon. Lack of this information restricts the understanding of the properties of the materials. In this paper, we report a Raman spectroscopy-based quantitative method to measure the free carbon concentration by using silicon as an external reference. We demonstrate that the technique provides a simple and reliable way for the carbon content quantification.
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Document Type: Research Article

Affiliations: 1: Advanced Materials Processing and Analysis Center, University of Central Florida, Orlando, Florida 32816, USA 2: Optical Tech Research Center, Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Science, Changchun 130032, China 3: National Key Laboratory of Thermostructure Composite Materials, Northwestern Polytechnical University,Xi'an, China 4: Department of Mechanical, Materials and Aerospace Engineering, University of Central Florida, Orlando, Florida 32816, USA

Publication date: October 1, 2009

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