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The Anorthite–Diopside System: Structural and Devitrification Study. Part II: Crystallinity Analysis by the Rietveld–RIR Method

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The crystallization behavior of 10 binary glasses belonging to the CaO–MgO–Al2O3–SiO2 quaternary system and two glasses corresponding to anorthite and diopside composition was investigated by X-ray diffraction, thermal, and thermomechanical analyses, and scanning electron microscopy. Particular emphasis is laid on the quantitative X-ray diffraction analysis by the Rietveld–reference intensity ratio combined procedure, which seems to be a useful tool to obtain time–temperature–transformation diagrams. Results showed that to obtain glass–ceramics with a significant crystalline phase presence, it is necessary to treat samples at 1000°C for 4 h or at 1100°C for 1 h.
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Document Type: Research Article

Affiliations: 1: Dipartimento di Ingegneria dei Materiali e dell'Ambiente, Facoltà di Ingegneria, Università di Modena e Reggio Emilia, 41100 Modena, Italy 2: Dipartimento di Scienze e Metodi dell'Ingegneria, Facoltà di Ingegneria, Università di Modena e Reggio Emilia, 42100 Reggio Emilia, Italy 3: DemoCenter s.c.a.r.l., 41100 Modena, Italy

Publication date: November 1, 2005

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