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Combustion Reaction During Mechanical Alloying Synthesis of Ti3SiC2 Ceramics from 3Ti/Si/2C Powder Mixture

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Mechanical alloying (MA) synthesis of Ti3SiC2 from a stoichiometric elemental powder mixture of Ti, Si, and C was conducted by using a planetary mill with a specially designed MA jar, which enables the real-time measurement of temperature and gas pressure during the MA process. Sudden gas pressure and temperature rises were detected when the mixed powders were mechanically alloyed for a certain period, and consequently a large amount of Ti3SiC2 particles was synthesized. Using the Ti–Si–C system as an example, the present study confirmed the combustion reaction triggered by the ball-milling process for the first time.
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Document Type: Research Article

Affiliations: 1: State Key Laboratory of New Ceramics and Fine Processing, Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, China 2: Department of Materials Processing, Graduate School of Engineering, Tohoku University, Sendai 980-8579, Japan

Publication date: May 1, 2005

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