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Solid-Solution Formation in the Synthesis of Fe-Zircon

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To investigate solid-solution formation in the iron-doped silicate (zircon) system, different samples were prepared by the ceramic method with addition of LiF as a mineralizer. The results of X-ray powder diffraction (XRD), 57Fe Mössbauer, and UV–visible spectroscopy showed that in the as-prepared samples, only a small fraction of iron, i.e., about 2.5 mol%, is hosted in the zircon structure as paramagnetic Fe3+ species, while the remaining Fe3+ cations form magnetic α-Fe2O3 particles that are trapped in the zircon matrix.
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Keywords: solid solutions; synthesis; zircon

Document Type: Research Article

Affiliations: 1: Programa de Ingeniería Molecular, Instituto Mexicano del Petróleo, Eje Central Lázaro C´rdenas 152, 07730 Mexico D.F., Mexico 2: DEPg., Facultad de Química, UNAM, Circuito Escolar, Cd. Universitaria, Coyoacan 04510, Mexico D.F., Mexico 3: Departamento de Química Inorgánica y Orgánica, Universitat Jaume I, Castellón 1208, Spain

Publication date: April 1, 2004

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