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trans-Di­aqua­bis­{2-[3-(di­methyl­amino)­prop-2-enoyl]­pyridine}­nickel(II) bis­(tetra­fluoro­borate) di­methyl­form­amide tetrasolvate

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The title compound, [Ni(C10H12N2O)2(H2O)2](BF4)2·4C3H7NO, was synthesized by the reaction of 2-[3-(di­methyl­amino)­prop-2-enoyl]­pyridine and Ni(BF4)2 in di­methyl­form­amide. It has been characterized by elemental analysis and X-ray diffraction techniques. The crystal structure reveals that the NiII atom, on an inversion center, has an NiN2O4 octahedral coordination environment with two carbonyl O atoms and two pyridyl N atoms in the equatorial plane and two water mol­ecules in the axial positions. 2-[3-(Di­methyl­amino)­prop-2-enoyl]­pyridine chelates to the Ni atom through the O and pyridine N atoms. Tetra­fluoro­borate counter-anions and di­methyl­form­amide solvent mol­ecules are not coordinated to the central metal ion.
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Document Type: Research Article

Publication date: December 1, 2004

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