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A cyclic dipalladium compound formed by concomitant N–C coupling and [2+3]-cyclo­addition: bis{-1-[4-(carbodiimido)­phenyl]­tetrazolato-2N:C5}bis­[bis­(tri­methyl­phosphine-P)­palladium(II)]

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The title compound, [Pd2(C8H4N6)2(C3H9P)4], was prepared by treating Pd(PMe3)2(N3)2 with 1,4-phenyl­ene diisocyanide [C6H4(NC)2]. This compound, a cyclic dimer, was formed by concomitant N—C coupling and [2 + 3]-cyclo­addition. Around the square-planar Pd atom, the carbodi­imide moiety and the tetrazolate ring are mutually trans. The N atom of the carbodi­imide moiety is bonded to the Pd center, and the five-membered tetrazolate ring is coordinated to the Pd atoms through the C atom. The molecule is located on a center of symmetry.
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Document Type: Research Article

Publication date: December 1, 2004

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