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Two polymorphs of tris(ethylenediamine)cobalt(III) tetrathioantimonate(V)

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Details of the structures of two polymorphs of tris(ethylenediamine)cobalt(III) tetrathioantimonate(V), [Co(C2H8N2)3][SbS4], are reported. The first polymorph crystallizes in the orthorhombic space group Pna21, whereas the second polymorph belongs to the tetragonal space group P42 bc. Both structures contain octahedral [Co(en)3]3+ cations (en is ethylenediamine) and tetrahedral [SbS4]3− anions, which are interconnected via various N—H...S hydrogen bonds to form two different types of three‐dimensional network.
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Document Type: Research Article

Affiliations: Key Laboratory of Inorganic Chemistry in Universities of Shandong, Department of Chemistry and Chemical Engineering, Jining University, Qufu, Shandong 273155, People's Republic of China

Publication date: August 15, 2013

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