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The interpenetrated three‐dimensional framework of a new mixed lithium/ammonium perchlorate grown in a gel medium

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Mixed lithium/ammonium perchlorate, Li0.41(NH4)0.59ClO4, has been prepared by gel diffusion using agar agar gel as the medium of growth at ambient temperature. The Cl and mixed Li/N atoms are located on the 4a () and 4b (, 0, ) special positions, respectively, in the space group I2d. The structure features a twofold interpenetrated three‐dimensional entanglement architecture, in which single three‐dimensional networks are constructed from tetrahedral coordination based on [–(ClO4)–(Li/NH4)–(ClO4)–] diamondoid arrays. A comparison of the crystal structures of Li0.41(NH4)0.59ClO4, LiClO4·3H2O, LiClO4 and NH4ClO4 is given.
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Document Type: Research Article

Affiliations: Laboratoire des Sciences des Matériaux et de l'Environnement, Faculté des Sciences de Sfax, Université de Sfax, 3000 Sfax, Tunisia

Publication date: April 15, 2013

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