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An Efficient Microwave-Promoted Solvent-Free α-Phosphoryloxylation of Ketones

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An efficient solvent-free α-phosphoryloxylation of ketones under microwave irradiation is reported. When ketones reacted with phosphates and (diacetoxyiodo)benzene under microwave irradiation for short time, the α-phosphoryloxylaction of ketones was easily be carried out and the corresponding ketol phosphates were prepared in moderate to good yields.
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Keywords: (Diacetoxyiodo)benzene; acetophenone; diphenyl; iodine; ketol phosphate; ketone; microwave irradiation; synthesis; water; α-Phosphoryloxylation

Document Type: Research Article

Publication date: September 1, 2012

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  • Letters in Organic Chemistry publishes original letters on all areas of organic chemistry including synthesis, bioorganic, medicinal, natural products, organometallic, supramolecular, molecular recognition and physical organic chemistry. The emphasis is placed on publishing quality papers very rapidly. Letters are processed rapidly and take full advantage of the Internet technology both for the submission and the review of the manuscripts.
    The journal is essential reading for all organic chemists both in academia and industry.
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