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Microwave-assisted Suzuki-Miyaura Cross-Coupling of Free (NH) 3-Bromoindazoles

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Suzuki-Miyaura cross-coupling of free (NH) indazoles is described. The reactions are carried out under microwave irradiation using various 3-bromoindazoles and boronic acids. Different reaction conditions were investigated and the best results were obtained using Pd(PPh3)4 and Cs2CO3 in a mixture of 1,4-dioxane/EtOH/H2O at 140 °C under microwave irradiation.
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Keywords: 3-chloroindazole; Boronic acids; Cs2CO3; Free (NH) indazoles; Indazoles; Microwave irradiation; Palladium-mediated cross-coupling; Pyridin-3-ylboronic acid; Sealed vessel; Suzuki-Miyaura cross-coupling

Document Type: Research Article

Publication date: 01 February 2013

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