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Synthesis of PbS and Ag2S Nanorods via Polyol Process

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PbS and Ag2S nanorods have been synthesized using a polyol process in the presence of poly(vinylpyrrolidone) (PVP). First, the production of Pb or Ag was realized via the thermal decomposition of a lead/silver salt. Then the Pb or Ag precursor was directly combined with S power under heating, leading to the formation of the final products. The samples were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy dispersive X-ray spectroscopy (EDS). PbS cubes and cubes with a hole in the center were prepared under different reaction conditions. Possible formation mechanisms of different PbS or Ag2S morphologies have briefly been discussed.
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Keywords: Ag2S; Cubes; Nanorods; PbS; Polyol Process; Synthesis

Document Type: Research Article

Affiliations: 1: Department of Chemistry of College of Pharmaceutical Sciences and Institute of Medicinal Chemistry, Hubei University of Medicine, Shiyan 442000, China 2: Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials and Ministry of Education Key Laboratory for Synthesis and Applications of Organic Functional Molecules, Hubei University, Wuhan 430062, China 3: Jiangsu Key Laboratory of Atmospheric Environment Monitoring and Pollution Control, Nanjing University of Information Science and Technology, Nanjing 210044, China

Publication date: August 1, 2018

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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