An Efficient Microwave-Promoted Solvent-Free α-Phosphoryloxylation of Ketones
An efficient solvent-free α-phosphoryloxylation of ketones under microwave irradiation is reported. When ketones reacted with phosphates and (diacetoxyiodo)benzene under microwave irradiation for short time, the α-phosphoryloxylaction of ketones was easily be carried out
and the corresponding ketol phosphates were prepared in moderate to good yields.
Keywords: (Diacetoxyiodo)benzene; acetophenone; diphenyl; iodine; ketol phosphate; ketone; microwave irradiation; synthesis; water; α-Phosphoryloxylation
Document Type: Research Article
Publication date: 01 September 2012
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