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Synthesis of TiO2 and TiO2-Pt and Their Application in Photocatalytic Degradation of Humic Acid

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ABSTRACT: 

The deposit of noble metal on titanium dioxide (TiO2) has been considered as an effective strategy to improve the activity of TiO2. In this study, TiO2 nanoparticles were prepared using a sol-gel route followed by heat treatment at elevated temperatures (573 K, 773 K, and 973 K). TiO2-Pt catalyst (1 wt%) was prepared by depositing Pt on the surface of the prepared TiO2 nanoparticles. TiO2 and TiO2-Pt were used as heterogeneous catalysts to remove humic acid with UV-light (120 W) illumination. TiO2 prepared at low temperature with smaller particle size and larger specific surface area had stronger activity on humic acid degradation. Deposit of Pt would favor separation of photogenerated charges and enhance the photocatalyst activity, but its coating of the active site also inhibited degradation of humic acid. The addition of H2O2 enhanced degradation of humic acid for more active oxygen produced. Low pH (pH = 4) was helpful to adsorb humic acid on the surface of TiO2 and, correspondingly, enhance degradation of humic acid (44.4%).
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Keywords: active site; humic acid; photocatalysis; platinum; titanium dioxide

Document Type: Research Article

Affiliations: State Key Laboratory of Pollution Control and Resource Reuse, College of Environmental Science and Engineering, Tongji University, Shanghai, China

Publication date: 2014-01-01

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    Water Environment Research (WER) publishes peer-reviewed research papers, research notes, state-of-the-art and critical reviews on original, fundamental and applied research in all scientific and technical areas related to water quality, pollution control, and management. An annual Literature Review provides a review of published books and articles on water quality topics from the previous year.

    Published as: Sewage Works Journal, 1928 - 1949; Sewage and Industrial Wastes, 1950 - 1959; Journal Water Pollution Control Federation, 1959 - Oct 1989; Research Journal Water Pollution Control Federation, Nov 1989 - 1991; Water Environment Research, 1992 - present.
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