Skip to main content

Analysis of pulp mill effluent contaminants in water, sediment, and fish muscle— chlorophenols and related compounds

Buy Article:

$30.00 plus tax (Refund Policy)

Abstract:

ABSTRACT:

The need for multimedia environmental studies on pulp mill effluent contaminants was addressed by refining and validating analytical protocols for the analysis of chlorinated phenols, guaiacols, catechols, phenolic aldehydes, and polymethoxybenzenes in water (µg/L range), sediment, and fish tissue samples (tenths of µ/g range). The methods, with common features for the different media, involved extraction with t-butyl methyl ether/dichloromethane solutions, with ascorbic acid added as an antioxidant. In the case of fish tissue, sample cleanup by size exclusion chromatography was carried out to reduce lipid interference. Derivatization with acetic anhydride /pyridine in organic solution yielded the acetates, which were analyzed by GC-SIM-MS. Excellent precision (SD = 2–15%) and satisfactory recoveries (42–115%) were achieved for most of the 32 contaminants evaluated. Application of these methods to samples from the northern Alberta region yielded satisfactory results (surrogate recoveries = 94–134%).

Keywords: analysis; chlororganics; chromatography; effluent; fish muscle; pulp mill; sediment

Document Type: Research Article

DOI: http://dx.doi.org/10.2175/WER.64.5.3

Publication date: July 1, 1992

More about this publication?
  • Water Environment Research® (WER®) publishes peer-reviewed research papers, research notes, state-of-the-art and critical reviews on original, fundamental and applied research in all scientific and technical areas related to water quality, pollution control, and management. An annual Literature Review provides a review of published books and articles on water quality topics from the previous year.

    Published as: Sewage Works Journal, 1928 - 1949; Sewage and Industrial Wastes, 1950 - 1959; Journal Water Pollution Control Federation, 1959 - Oct 1989; Research Journal Water Pollution Control Federation, Nov 1989 - 1991; Water Environment Research, 1992 - present.
  • Editorial Board
  • Information for Authors
  • Submit a Paper
  • Subscribe to this Title
  • Membership Information
  • Information for Advertisers
  • WEF Bookstore
  • Ingenta Connect is not responsible for the content or availability of external websites
wef/wer/1992/00000064/00000005/art00003
dcterms_title,dcterms_description,pub_keyword
6
5
20
40
5

Access Key

Free Content
Free content
New Content
New content
Open Access Content
Open access content
Subscribed Content
Subscribed content
Free Trial Content
Free trial content
Cookie Policy
X
Cookie Policy
Ingenta Connect website makes use of cookies so as to keep track of data that you have filled in. I am Happy with this Find out more