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Odor Assessor Performance to Reference and Non-Reference Odorants

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The European Standard test method for the determination of odor concentrations (EN13725:2003) is based on the standardization of the assessors (test subjects) with a known sensitivity to an accepted reference odorant, n-butanol. The assumption is made that the sensitivity for the reference will be a predictor for sensitivity to other substances, i.e. non-reference odorants, odorant mixtures, and environmental odors.

Assessors from a commercial odor laboratory, certified to the EN13725 selection criteria, tested hydrogen sulfide as a non-reference odorant. Hydrogen sulfide was used as the non-reference odorant representing a common compound that is found in wastewater process odors and odors from various other industries, e.g. pulp and paper, landfill, agriculture. This paper analyzes the following:

Comparison of individual assessor responses to n-butanol and hydrogen sulfide during a test session;

Comparison of the odor panel results for n-butanol and hydrogen sulfide during a test session;

Comparison of assessor performance testing with n-butanol and hydrogen sulfide; and

Comparison of panel performance testing with n-butanol and hydrogen sulfide.

The first two objectives compare results obtained during any one test session through review of individual assessor responses and the panel average as a whole. The second two objectives will illustrate the repeatability of the individual assessors and the odor panel as a group by providing statistical evidence of parameters for accuracy and precision.

EN13725 provides a framework for monitoring accuracy and precision of results in an olfactometry laboratory. Regular testing of the reference odorant n-butanol allows a laboratory to quantify these parameters. Periodic testing can also be performed on non-reference odor samples, e.g. hydrogen sulfide, to confirm these parameters as part of a comprehensive QA/QC program. This statistical information provides a user of odor testing results greater understanding of the meaning and application of these results.

Keywords: ASTM E679; EN13725; H2S; Olfactometry; butanol; detection threshold; hydrogen sulfide; n-butanol; odor thresholds

Document Type: Research Article


Publication date: January 1, 2010

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