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Home / Synthetic Communications, Volume 40, Number 5

General and Efficient Synthesis of O-Sulfonylhydroxylamine Derivatives

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Authors: Qin, Liqiong; Zhou, Zhiming; Wei, Jia; Yan, Ting; Wen, Hongliang

Source: Synthetic Communications, Volume 40, Number 5, January 2010, pp. 642-646(5)

Publisher: Taylor and Francis Ltd

DOI: https://doi.org/10.1080/00397910903007111

A general and efficient synthetic route to O-sulfonylhydroxylamine derivatives is described. The approach involves acylation of hydroxylamine with benzyl chloroformate to give N-carbobenzoxy hydroxylamine, followed by sulfonation and hydrogenolysis to give products.

Keywords: Benzyl chloroformate; O-sulfonylhydroxylamine derivatives; hydrogenolysis; sulfonation

Document Type: Research Article

Affiliations: School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, China

Publication date: 01 January 2010

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