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Home / Synthetic Communications, Volume 39, Number 13

Solvent- and Catalyst-Free Synthesis of New Unsymmetrical Multidentate Thio-bis-aminophenol Ligands by Mannich Condensation

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Authors: Shockravi, Abbas 1 ; Sadeghpour, Mahdieh 2 ; Olyaei, Abolfazl 3 ; 

Source: Synthetic Communications, Volume 39, Number 13, January 2009, pp. 2347-2359(13)

Publisher: Taylor and Francis Ltd

DOI: https://doi.org/10.1080/00397910802654823

A one-pot, three-component, Mannich condensation of electron-rich aromatic compounds such as 5-methyl-2-hydroxyphenyl sulfide, 2-aminopyrimidine, and various aromatic aldehydes were used to prepare a series of new unsymmetrical multidentate aminophenol ligands. These compounds were synthesized in solvent-free conditions as a fast, simple, convenient, and uncatalyzed method. Details of the reaction conditions are discussed.

Keywords: Aminophenol; Mannich; multidentate; solvent-free; unsymmetrical

Document Type: Research Article

Affiliations: 1: Faculty of Chemistry, Tarbiat Moallem University, Tehran, Iran 2: Faculty of Chemistry, Tarbiat Moallem University, Tehran, Iran,Department of Chemistry, Islamic Azad University, Takestan Branch, Qazvin, Iran 3: Department of Chemistry, Payame Noor University, Qazvin, Iran

Publication date: 01 January 2009

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