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Chlorodimethylsulfonium Chloride-Mediated Formation of Phenyl-α-chloroazoalkanes

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Abstract:

Phenylhydrazones (1) are efficiently converted into phenyl-α-chloroazoalkanes (2) upon treatment with chlorodimethylsulfonium chloride. Pendent olefins, silyl ethers, and the phenyl ring of the hydrazone are stable to these reaction conditions.

Keywords: Activated DMSO; aryl-α-chloroazoalkanes; chlorodimethylsulfonium chloride; hydrazone; oxidation; phenylhydrazone

Document Type: Research Article

DOI: https://doi.org/10.1080/00397910802179961

Affiliations: Department of Chemistry, University of Vermont, Bington, Vermont, USA

Publication date: 2008-01-01

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