Chlorodimethylsulfonium Chloride-Mediated Formation of Phenyl-α-chloroazoalkanes
Phenylhydrazones (1) are efficiently converted into phenyl-α-chloroazoalkanes (2) upon treatment with chlorodimethylsulfonium chloride. Pendent olefins, silyl ethers, and the phenyl ring of the hydrazone are stable to these reaction conditions.
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