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Synthesis of Thiourea‐Bridged Cluster Glycoside Calixarenes

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Thiourea-bridged peracetylated glycoside calixarenes have been smoothly synthesized by the addition reactions of tetraacetylglycosyl isothiocyanates with amidoamine derivatives of calix[4]resorcinarene and p-tert-butylcalix[n]arenas ( n =6, 8) in high yields (40–75%). All the glycoside-containing calixarenes were characterized by 1 H NMR, IR spectroscopy, and elemental analysis.
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Keywords: Calixarene; calix[4]resorcinarene; glycoside; isothiocyanate; thiourea

Document Type: Research Article

Affiliations: College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, China

Publication date: 01 January 2005

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