Analysis of X-Ray Diffraction Line Profiles of Lead Zirconate Titanate Using the Fourier Method

Authors: W. THAMJAREE¹; W. NHUAPENG¹; T. TUNKASIRI¹

Source: Ferroelectrics Letters Section, Volume 31, Numbers 3-4, Numbers 3-4/2004 , pp. 79-85(7)

Publisher: Taylor and Francis Ltd

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Abstract:

Lead zirconate titanate (PZT) powder was prepared by a solid state reaction. The X-ray line broadening produced in PZT powder was analyzed by the Fourier method to estimate particle size and microstrain. It was found that an increase of the annealing temperature caused the microstrain to decrease owing to an increase in particle size. The Scherrer formula used to calculate the particle size yielded considerably smaller values.

Keywords: PZT; particle; Fourier method

Document Type: Research article

DOI: 10.1080/07315170490480975

Affiliations: 1: Department of Physics, Faculty of Science, Chiangmai University Chiangmai 50200 Thailand

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