Authors: Nicholls, J.R.; Bennett, M.J.

Source: Materials at High Temperatures, Volume 17, Number 3, August 2000 , pp. 413-428(16)

Publisher: Science Reviews 2000 Ltd

Abstract:

This paper reviews current procedures used for cyclic oxidation testing and their ability to simulate service behaviour for life time prediction modelling. Test complexity varies from a simple laboratory, slow cycle, furnace test to the use of high velocity dynamic combustion rigs. It is shown that the response of an alloy under cyclic oxidation testing varies, depending on the exact test conditions chosen and the length of test exposure, but for many alloy systems this response has common features. It is proposed that all alloys that are protected by a stable, slow growing oxide scale conform to a common, generic behaviour under cyclic oxidation conditions. This life cycle of such alloys involves first the formation of a stable, protective oxide. At a critical thickness this may start to spall, increasing the rate of scale forming element consumption. When the activity of such elements falls below a critical level, in the near surface region, internal oxidation results together with the formation of less protective scales. Ultimately, it is no longer possible for the alloy to self repair following a thermal cycle and then breakaway corrosion ensures, marking the end of the alloys life.

Thus the choice of cyclic test procedure must be tailored to the particular phase of the alloy life cycle under investigation.

Keywords: cyclic oxidation testing

Document Type: Research article

DOI: http://dx.doi.org/10.3184/096034000783640758

Affiliations: 1: Cranfield University, Cranfield, Bedfordshire MK43 0AL, UK

Publication date: 2000-08-15

More about this publication?

• Materials at High Temperatures serves the needs of those who develop and use materials for high temperature applications. It publishes peer reviewed contributions relating to high temperature applications in the power, chemical, engine, processing and furnace industries.

  The effects of high temperatures on corrosion, fatigue, creep, strength and wear in alloys, intermetallics, ceramics, refractories and composites are covered. Papers dealing with aspects of materials usage including modelling of behaviour and life prediction will be particularly welcome. The journal has a policy of emphasizing practical aspects and authors presenting results from research programmes are encouraged to relate these, if possible, to actual or potential applications.

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