Two-Dimensional Vibrational Correlation Spectroscopic Study on the Crystallization Process of Poly(ethylene-2,6-naphthalate)

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Abstract:

Conformation changes during the crystallization process of poly(ethylene-2,6-naphthalate), including the induction period, were investigated by means of generalized two-dimensional correlation spectroscopy. A broad carbonyl stretching vibration band, as well as a broad band for a naphthalene ring vibration, was resolved in terms of the coplanarity of the carbonyl and the naphthalene ring. A difference in conformation change was found between cold crystallization and melt crystallization.

Keywords: CRYSTALLIZATION PROCESS; FT-IR SPECTROSCOPY; POLY(ETHYLENE-2,6-NAPHTHALATE); TWO-DIMENSIONAL VIBRATIONAL CORRELATION SPECTROSCOPY

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702001950706

Affiliations: 1: Nicolet Japan Corporation, 3-9-13 Moriya, Kanagawa-ku, Yokohama, 221-0022, Japan 2: Department of Applied Chemistry, Faculty of Engineering, Tokyo Metropolitan University, 1-1 Minami-ohsawa, Hachioji, Tokyo 192-0397, Japan

Publication date: July 1, 2000

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