XPS Study of a New Heterogeneous Ruthenium Catalyst Precursor

Authors: Smet, P.; Verpoort, F.; Doncker, G. De; Bossuyt, A. R.; Fiermans, L.; Verdonck, L.

Source: Applied Spectroscopy, Volume 51, Issue 12, Pages 450A-455A and 1769-1953 (December 1997) , pp. 1807-1813(7)

Publisher: Society for Applied Spectroscopy

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Abstract:

The catalyst precursor has been synthesized by modifying the silica surface with ClPPh2 followed by a surface reaction with RuCl3. Sup- ports consisting of a thin layer of SiO2 on a silicon single crystal have been used. Characterization of the different stages in the reaction procedure has been performed by a combination of conventional and angle-resolved X-ray photoelectron spectroscopy (XPS) using RuCl3/P(C6H5)2/SiO2/Si(100) model precursors. Different types of ruthenium centra have been identified.
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