In Situ Spectroscopic Study of Microwave Polymerization

Authors: Stellman, Christopher M.; Aust, Jeffrey F.; Myrick, Michael L.

Source: Applied Spectroscopy, Volume 49, Issue 3, Pages 267-402 (March 1995) , pp. 392-394(3)

Publisher: Society for Applied Spectroscopy

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Abstract:

Microwaves provide a commercially advantageous method of rapidly curing polymeric samples. Curing times of several hours with traditional ovens are easily reduced to several minutes by microwave curing. Many commonly used sample monitoring probes (e.g., thermocouples) contain metallic elements that are incompatible with microwave processing. Such accelerated polymer processing via rapid microwave heating would benefit from rapid in situ monitoring techniques using optical spectroscopy.

Keywords: Chemometrics; Fiber optic spectroscopy; Microwave polymerization; Raman spectroscopy

Document Type: Short Communication

DOI: http://dx.doi.org/10.1366/0003702953963535

Affiliations: Department of Chemistry, University of South Carolina, Columbia, South Carolina 29208

Publication date: March 1, 1995

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