Simultaneous Detection of Optical Isomers and the Separation of Overlapping Resonances in a 1H NMR Spectrum of (+/-)-2,2-Dimethyl-1-Phenyl-1-Propanol Using an NMR Shift Reagent

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Abstract:

The enantiomer separation and the spectral simplification of overlapped resonances in a high-resolution 1H NMR spectrum of a model compound have been successfully accomplished with the use of paramagnetic shift reagent. Both 1H and 13C NMR have been applied to determine the composition of a mixture containing optically active enantiomers of (+/-)-2,2-dimethyl-1-phenyl-1-propanol.

Keywords: NMR; Optical isomers, detection; Shift reagent; Spectroscopic techniques

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702894203471

Affiliations: The BOC Group, Inc., Technical Center, Murray Hill, New Jersey 07974

Publication date: September 1, 1989

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