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Micro-Raman Spectroscopy of Selected Solid UxOyFz Compounds

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Abstract:

Micro-Raman spectroscopy has been utilized to examine the spectra of solid samples of α-UF5, β-UF5, UF6, three types of UO2F2, the powder residue from a static UF6 release, and γ-UO3. The spectra are presented and compared to previous literature values, with new features indicated where appropriate. With the implied constraint of proper sample handling, micro-Raman spectroscopy is a useful technique for the ready identification of uranium fluorides, oxyfluorides, and oxides.

Keywords: Micro-Raman spectroscopy; UF6 release, UF6 hydrolysis; Uranium hexafluoride; Uranium pentafluoride; Uranium trioxide; Uranyl fluoride

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702894203002

Affiliations: 1: Oak Ridge Gaseous Diffusion Plant, Materials and Chemistry Technology Department, P.O. Box 2003, Oak Ridge, Tennessee 37831-7271 2: Chemistry Department, University of Tennessee, Knoxville, Tennessee 37966

Publication date: March 1, 1989

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